Molecular Biophysics and Soft Matter
 
 
Facilities


Atomic Force Microscope
Time-resolved luminescence
Confocal and two photon microscope

Raman spectrometers
IR spectrometer
OA and PL spectrometers
Light scattering nano sizer
Sample preparation laboratory
Helium liquefier

 

External facilities


TEM
SEM

 

DiFi facilities


Reactor
VUV spectrometer
Laser and in situ OA
EPR spectrometer
Circular dichroism

 


Helium Liquefier Laboratory

DiFi Laboratory
Laboratory directed by: Prof. Roberto Boscaino

The helium liquefier consists of a liquefier module (KOCH Mod.1410) (left photo with Mr G. Lapis and Mr G. Napoli)  and a compressor module (two compressors KOCH Mod. 1400) (right photo with Mr G. Napoli and Mr F. Testaino).  The liquid production rate is 20 liters/h in steady state operation, using both compressors and liquid nitrogen pre-cooling.

 


 

 
 


Operating Principle
: In operation helium gas is compressed (compressor module) and delivered to the liquefier module. The gas is cooled in the liquefier by heat transfer in the heat exchanger , by work extraction in the expansion engine, and, finally, by expansion in the Joule-Thomson valve. All these processes take place in a high-vacuum chamber. The liquid helium produced is delivered to an externally located dewar via a coaxial delivery tube. Initial pre-cooling by liquid nitrogen is optional (heat echanger not shown in the diagram).


 
 
 
 


In the real set-up, the liquefier module includes two heat exchangers and two expansion engines. It is fed by two compressors. In steady state operation the temperature at the output of the first expansion engine is nearly 20 K and at the output of the second engine is nearly 7 K. The liquid production is nearly 20 liters/h, if liquid nitrogen pre-cooling is used.

 

This laboratory is integrated in MeSIAM - Regional Laboratory of CNISM